Analytical systems for synchrotrons

XANELS XPS ultra high vacuum system [project 043]

Description

UHV system designed to operate as both a stand-alone device or as an end station in synchrotron installations. A key feature of the system is the ability to handle volatile samples throughout via efficient liquid nitrogen cooling. This is a fundamental design feature of this specific system for reproducible studies of volatile mineral samples.

Specification

The system is a multi-user XANELS and XPS faci­lity characterised by the following features:

  • High throughput photoemission energy analyser
  • NEXAFS detector (partial electron yield and total flu­orescence yield)
  • Sample cooling to 120K (using LN2) or ~40K (using LHe)
  • Flood gun and dual-anode X-ray source
  • Ability to transfer samples at 120K
  • Rotary distribution chamber allows sample transfer to 8 chambers
  • Fast sample entry load-lock with glove-box
  • Sample fracture chamber and storage cham­ber
  • Preparation chamber for sputtering, evaporation etc.
  • Ability to be upgraded via add-on chambers using spare-ports
  • Motorised sample manipulators and user friendly control system
  • Support frame with a large range of adjustment, to allow SXSI to be mounted on the complete range of NSRRC soft X-ray beamlines, and on the Australian Syn­chrotron.

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» Components

Analytical Chamber

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Designed for applications requiring the investigation of the chemical and physical properties of solid state surfaces, thin films and nanomaterials.

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Cleaver Chamber

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The cleaver chamber provides a UHV environment for cleaving crystal specimens.

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Effusion Cell EF 40C1

» Effusion Cell EF 40C1

EF 40C1 Effusion Cell (Knudsen Cell) is a source designed for indirect resistive heating and delivering highly constant evaporation rates.

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Electron beam evaporator EBV 40A1

» Electron beam evaporator EBV 40A1

The electron beam evaporator EBV 40A1 is designed for ultra-pure sub-monolayer and multilayer MBE thin film growth.

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Ion Source IS 40C1

» Ion Source IS 40C1

Compact, easy-to-use extractor type ion gun for sample surface cleaning.

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Ion Source IS 40E1

» Ion Source IS 40E1

Two lens, extractor type, focused and differentially pumped ion gun.

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Load Lock Chamber

» Load Lock Chamber

Provides a fast and clean method of introducing samples into UHV systems.

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Preparation Chamber

» Preparation Chamber

For standard sample preparation techniques, thin film growth, sputtering, annealing and advanced preparation techniques with in-situ characterisation.

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Radial Distribution Chamber (UFO)

» Radial Distribution Chamber (UFO)

Designed to transfer samples between multiple analysis, deposition or preparation chambers that are connected to it.

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Storage Chamber

» Storage Chamber

The storage chambers allow storage of up to 10 sample holders under UHV conditions.

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X-ray Source RS 40B1

» X-ray Source RS 40B1

High intensity twin anode Al/Mg source optimized for XPS and high pressure XPS experiments.

 
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PTS STANDARD sample holder

» PTS STANDARD sample holder

The PTS STANDARD sample holder for easy sample mounting and optional BIAS current measurement.

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PTS POWDER sample holder

» PTS POWDER sample holder

The PTS POWDER SAMPLE HOLDER is designed for powder samples that do not require heating or cooling.

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PTS BASE CONTAINER sample holder

» PTS BASE CONTAINER sample holder

The PTS BASE CONTAINER SAMPLE HOLDER is designed as an adapter to accept samples up to 50mm diameter and 7.5mm thick.

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PTS 1000 RES/C-K sample holder

» PTS 1000 RES/C-K sample holder

The PTS 1000 RES/C-K sample holder has indirect (resistive) sample heating up to 1000°C and cooling to –170°C.

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PTS 1000 RES/C WITH EXTRA CONTACT sample holder

» PTS 1000 RES/C WITH EXTRA CONTACT sample holder

PTS 1000 RES/C-K sample holder with extra contacts is specifically for use in the MBE Chamber.

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PTS 1200 EB/C-K Mo sample holder

» PTS 1200 EB/C-K Mo sample holder

The PTS 1200 EB/C-K Mo sample holder features electron beam sample heating up to 1200°C, and cooling to –180°C.

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PTS 2000 EB/C-C sample holder

» PTS 2000 EB/C-C sample holder

The PTS 2000 EB/C-C sample holder features electron beam sample heating up to 2000°C and is designed specifically for high temperature experiments.

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PTS 1200 DIR/C-K sample holder

» PTS 1200 DIR/C-K sample holder

The PTS with Direct Heating holder allows direct heating of the sample up to 1200°C and cooling down to -170°C.

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PTS 700/-90 HPC RES/C-K RG sample holder

» PTS 700/-90 HPC RES/C-K RG sample holder

The PTS HPC RES/C-K RG sample holder is dedicated for the High Pressure Cell (reactor).

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PTS 700/-90 HPC RES/C-K RG PS sample holder

» PTS 700/-90 HPC RES/C-K RG PS sample holder

The PTS HPC RES/C-K RG Sample Holder is for high pressure, reactive gas studies of powdered catalyst samples.

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PTS CLEAV RES/C-K sample holder

» PTS CLEAV RES/C-K sample holder

The PTS CLEAV RES/C-K is specifically designed for sample cleaving.

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PTS CLEAV sample holder

» PTS CLEAV sample holder

The PTS CLEAV Sample Holder is a version of the PTS CLEAV RES/C-K holder without heating or cooling capabilities.

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PTS 1000 IR RES/C-K sample holder

» PTS 1000 IR RES/C-K sample holder

The PTS 1000 IR RES/C-K Sample Holder is designed specifically for optical transmission spectroscopy (IR, UV) over the temperature range –170°C to 1000°C.

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PTS 1000 OMC RES/C-K sample holder

» PTS 1000 OMC RES/C-K sample holder

The PTS 1000 OMC RES/C-K sample holder adapts to flag style sample holders for systems that are equipped with STM.

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PTS 1400 OMC EB/C-K sample holder

» PTS 1400 OMC EB/C-K sample holder

The PTS 1400 OMC EB/C-K sample holder adapts to flag style sample holders for systems that are equipped with STM.

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PTS 1200 RHK EB/C-K sample holder

» PTS 1200 RHK EB/C-K sample holder

The PTS 1200 RHK EB/C-K sample holder has indirect sample heating up to 1200°C and cooling down to –170°C.

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PTS SPM DIR/C-K sample holder

» PTS SPM DIR/C-K sample holder

The PTS SPM DIR/C-K Sample Holder is for SPM work and is equipped with direct sample heating and cooling over the range -170°C to 1200°C.

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PTS SPM CLEAV sample holder

» PTS SPM CLEAV sample holder

The PTS SPM Cleav sample holder combines sample cleaving capabilities with SPM compatibility over the temperature range -170°C to 600°C (indirectly heated).

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PTS SPM 2000 EB/C-C sample holder

» PTS SPM 2000 EB/C-C sample holder

The PTS SPM 2000 EB/C-C sample holder is for SPM work and is equipped with electron beam sample heating up to 2000°C.

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PTS QUARTZ sample holder

» PTS QUARTZ sample holder

The PTS QUARTZ sample holder is equipped with integrated quartz balance for deposition rate measurements.

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PTS FARA sample holder

» PTS FARA sample holder

The PTS FARA sample holder has integrated Faraday Cup with secondary electron suppressor for beam profile measurements.

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PTS FARA EXTRA CAPABILITY sample holder

» PTS FARA EXTRA CAPABILITY sample holder

The PTS Faraday Cup with extra capability Sample Holder has replaceable aperture plates.

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PTS 200 RES sample holder

» PTS 200 RES sample holder

The PTS 200 RES sample holder features a heated, rotating wire of 129mm L and 0.5mm dia (max) for vapor deposition experiments.

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Flag style sample holders

» Flag style sample holders

Commonly used sample holder for a wide range of applications.

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Deposition holders

» Deposition holders

Sample holders (substrate holders, plates, wafers, molyblocs) dedicated for different deposition techniques, such as MBE, magnetron sputtering, thermal evaporation and others.

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» Electronics

Bakeout Control Unit BCU14

» Bakeout Control Unit BCU14

Perfect unit dedicated for heating zones of the vacuum systems as well as heating samples inside the preparation chambers.

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Electron Beam Evaporator Power Supply EBV40A-PS

» Electron Beam Evaporator Power Supply EBV40A-PS

Designed for supplying Electron Beam Evaporator EBV40A used for evaporation of materials under UHV conditions.

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Titanium Sublimation Pump Power Supply TSP03-PS

» Titanium Sublimation Pump Power Supply TSP03-PS

For constant filament current operation and features a thyristor and phase-control circuit for long-term and trouble-free TSP operation.

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X-ray Source Electronics Set XR40B

» X-ray Source Electronics Set XR40B

XR40B electronics set is used to control the X-ray source RS 40B1.

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See more  ›

» One axis manipulators

Z Chain Slide

» Z Chain Slide

The Z Chain Slide provides short strokes of Z travel with a wide range of bellows I.D.

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Z Slide

» Z Slide

The Z Slide is a precision, high rigidity UHV specimen translator having Z motion.

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See more  ›

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